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[PMID]: | 27356382 |
[Au] Autor: | Ding JH; Yuan MM; Yu Y; Zhou GP |
[Ti] Título: | [Ethyl Acetate-Soluble Chemical Constituents from Callicarpa kwangtungensis (II)]. |
[So] Source: | Zhong Yao Cai;38(11):2314-7, 2015 Nov. | [Is] ISSN: | 1001-4454 |
[Cp] País de publicação: | China |
[La] Idioma: | chi |
[Ab] Resumo: | OBJECTIVE: To study the ethyl acetate-soluble chemical constituents of Callicarpa kwangtungensis. METHODS: The chemical constituents were isolated by column chromatography on silica gel, Sephadex LH-20 and MPLC. Their chemical structures were elucidated on the basis of special analysis. RESULTS: Eleven compounds were isolated from the ethyl acetate-soluble part of Callicarpa kwangtungensis, whose structures were elucidated as 4-methoxybenzoic acid (1), 3,4-dihydroxybenzoic acid (2), 4-hydroxy cinnamic acid(3), phenyl-ß-D-glucopyranoside (4), 3,4,5-trimethoxyphenyl-ß-D-glucopyranoside (5), 2α,3ß,22ß,23-tetrahydroxyursolic-12-en-28-oic acid (6), 2α,3ß,6ß,19α-tetrahydroxy-urs-12-en-28-O-ß-D-glucopyranoside (7), 2ß,3ß,6ß,16α-tetrahydroxy-olean-12-en-28-O-ß-D-glucopyranoside (8), (3S, 6E, 10R)-10-ß-D-glucopyranosyloxy-3,11-dihydroxy-3,7,11-trimethyldodeca-1,6-diene (9), icariside C5(10), and (2E, 6E)-10-ß-D-glucopyranosyl-1, 11-dihydroxy-3, 7, 11-trimethyldodeca-2,6-diene (11). CONCLUSION: Compounds 4 - 11are isolated from Callicarpa genus for the first time, compounds 1 - 3 are isolated from this plant for the first time. |
[Mh] Termos MeSH primário: |
Callicarpa/química Compostos Fitoquímicos/análise
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[Mh] Termos MeSH secundário: |
Acetatos Cromatografia Compostos Fitoquímicos/isolamento & purificação
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[Pt] Tipo de publicação: | ENGLISH ABSTRACT; JOURNAL ARTICLE |
[Nm] Nome de substância:
| 0 (Acetates); 0 (Phytochemicals); 76845O8NMZ (ethyl acetate) |
[Em] Mês de entrada: | 1607 |
[Cu] Atualização por classe: | 160630 |
[Lr] Data última revisão:
| 160630 |
[Sb] Subgrupo de revista: | IM |
[Da] Data de entrada para processamento: | 160701 |
[St] Status: | MEDLINE |
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