Base de dados : MEDLINE
Pesquisa : D01.268.556.793 [Categoria DeCS]
Referências encontradas : 2705 [refinar]
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  1 / 2705 MEDLINE  
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[PMID]:28731418
[Au] Autor:Pérez González EL; Medina Alfaro I; Iglesias Cadarso A; Boteanu C
[Ad] Endereço:Allergy Section, Hospital Universitario Puerta de Hierro, Majadahonda, Spain.
[Ti] Título:An Unusual Case of Contact Dermatitis Caused by a Pacemaker Implanted for Neurostimulation.
[So] Source:J Investig Allergol Clin Immunol;27(4):272-273, 2017.
[Is] ISSN:1018-9068
[Cp] País de publicação:Spain
[La] Idioma:eng
[Mh] Termos MeSH primário: Dermatite Alérgica de Contato/etiologia
Nervo Obturador
Marca-Passo Artificial/efeitos adversos
Ródio/efeitos adversos
Silicones/efeitos adversos
[Mh] Termos MeSH secundário: Adulto
Seres Humanos
Neuroestimuladores Implantáveis
Masculino
Testes Cutâneos
[Pt] Tipo de publicação:CASE REPORTS; JOURNAL ARTICLE
[Nm] Nome de substância:
0 (Silicones); DMK383DSAC (Rhodium)
[Em] Mês de entrada:1708
[Cu] Atualização por classe:170831
[Lr] Data última revisão:
170831
[Sb] Subgrupo de revista:IM
[Da] Data de entrada para processamento:170722
[St] Status:MEDLINE
[do] DOI:10.18176/jiaci.0168


  2 / 2705 MEDLINE  
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[PMID]:28521262
[Au] Autor:Jardim GAM; Silva TL; Goulart MOF; de Simone CA; Barbosa JMC; Salomão K; de Castro SL; Bower JF; da Silva Júnior EN
[Ad] Endereço:Institute of Exact Sciences, Department of Chemistry, Federal University of Minas Gerais, CEP 31270-901, Belo Horizonte, MG, Brazil.
[Ti] Título:Rhodium-catalyzed C-H bond activation for the synthesis of quinonoid compounds: Significant Anti-Trypanosoma cruzi activities and electrochemical studies of functionalized quinones.
[So] Source:Eur J Med Chem;136:406-419, 2017 Aug 18.
[Is] ISSN:1768-3254
[Cp] País de publicação:France
[La] Idioma:eng
[Ab] Resumo:Thirty four halogen and selenium-containing quinones, synthesized by rhodium-catalyzed C-H bond activation and palladium-catalyzed cross-coupling reactions, were evaluated against bloodstream trypomastigotes of T. cruzi. We have identified fifteen compounds with IC /24 h values of less than 2 µM. Electrochemical studies on A-ring functionalized naphthoquinones were also performed aiming to correlate redox properties with trypanocidal activity. For instance, (E)-5-styryl-1,4-naphthoquinone 59 and 5,8-diiodo-1,4-naphthoquinone 3, which are around fifty fold more active than the standard drug benznidazole, are potential derivatives for further investigation. These compounds represent powerful new agents useful in Chagas disease therapy.
[Mh] Termos MeSH primário: Técnicas Eletroquímicas
Quinonas/farmacologia
Ródio/química
Tripanossomicidas/farmacologia
Trypanosoma cruzi/efeitos dos fármacos
[Mh] Termos MeSH secundário: Animais
Catálise
Relação Dose-Resposta a Droga
Macrófagos/efeitos dos fármacos
Camundongos
Estrutura Molecular
Quinonas/síntese química
Quinonas/química
Relação Estrutura-Atividade
Tripanossomicidas/síntese química
Tripanossomicidas/química
[Pt] Tipo de publicação:JOURNAL ARTICLE
[Nm] Nome de substância:
0 (Quinones); 0 (Trypanocidal Agents); DMK383DSAC (Rhodium)
[Em] Mês de entrada:1709
[Cu] Atualização por classe:170926
[Lr] Data última revisão:
170926
[Sb] Subgrupo de revista:IM
[Da] Data de entrada para processamento:170519
[St] Status:MEDLINE


  3 / 2705 MEDLINE  
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[PMID]:28387441
[Au] Autor:Großeheilmann J; Kragl U
[Ad] Endereço:Department of Chemistry, University of Rostock, Albert-Einstein-Str. 3a, 18059, Rostock, Germany.
[Ti] Título:Simple and Effective Catalyst Separation by New CO -Induced Switchable Organocatalysts.
[So] Source:ChemSusChem;10(12):2685-2691, 2017 Jun 22.
[Is] ISSN:1864-564X
[Cp] País de publicação:Germany
[La] Idioma:eng
[Ab] Resumo:CO -induced switchable tertiary amine-based organocatalysts were investigated for an efficient catalyst and product separation by its different partitioning between an organic and carbonated water phase. In this case study, the switching ability of eight tertiary amine-based catalysts between the organic and water phase by addition or removal of CO was investigated. Here, the catalyst switched both nearly completely (99.9 %) into the aqueous phase by addition of CO and effectively back into the organic phase (99.3 %) by expelling CO . With this technique, the organocatalyst was successfully recovered and reused twelve times without significant loss of activity (up to 90 % enantiomeric excess) for the asymmetric nitroaldol (Henry) reaction. After the first catalyst switch, evaporation of the solvent affords the product in 98 % purity without any further purification steps.
[Mh] Termos MeSH primário: Aminas
Dióxido de Carbono/química
Dióxido de Carbono/isolamento & purificação
Compostos Orgânicos/química
[Mh] Termos MeSH secundário: Aminas/química
Catálise
Cobalto/química
Compostos Organometálicos/química
Ródio/química
Solventes/química
[Pt] Tipo de publicação:JOURNAL ARTICLE
[Nm] Nome de substância:
0 (Amines); 0 (Organic Chemicals); 0 (Organometallic Compounds); 0 (Solvents); 142M471B3J (Carbon Dioxide); 3G0H8C9362 (Cobalt); DMK383DSAC (Rhodium)
[Em] Mês de entrada:1707
[Cu] Atualização por classe:170726
[Lr] Data última revisão:
170726
[Sb] Subgrupo de revista:IM
[Da] Data de entrada para processamento:170408
[St] Status:MEDLINE
[do] DOI:10.1002/cssc.201700491


  4 / 2705 MEDLINE  
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[PMID]:28338642
[Au] Autor:Han Q; Huo Y; Wu J; He Y; Yang X; Yang L
[Ad] Endereço:School of Chemical Engineering, Xi'an University, Xi'an 710065, China. xahquan@hotmail.com.
[Ti] Título:Determination of Ultra-trace Rhodium in Water Samples by Graphite Furnace Atomic Absorption Spectrometry after Cloud Point Extraction Using 2-(5-Iodo-2-Pyridylazo)-5-Dimethylaminoaniline as a Chelating Agent.
[So] Source:Molecules;22(4), 2017 Mar 24.
[Is] ISSN:1420-3049
[Cp] País de publicação:Switzerland
[La] Idioma:eng
[Ab] Resumo:A highly sensitive method based on cloud point extraction (CPE) separation/preconcentration and graphite furnace atomic absorption spectrometry (GFAAS) detection has been developed for the determination of ultra-trace amounts of rhodium in water samples. A new reagent, 2-(5-iodo-2-pyridylazo)-5-dimethylaminoaniline (5-I-PADMA), was used as the chelating agent and the nonionic surfactant TritonX-114 was chosen as extractant. In a HAc-NaAc buffer solution at pH 5.5, Rh(III) reacts with 5-I-PADMA to form a stable chelate by heating in a boiling water bath for 10 min. Subsequently, the chelate is extracted into the surfactant phase and separated from bulk water. The factors affecting CPE were investigated. Under the optimized conditions, the calibration graph was linear in the range of 0.1-6.0 ng/mL, the detection limit was 0.023 ng/mL for rhodium and relative standard deviation was 3.67% ( = 1.0 ng/mL, = 11).The method has been applied to the determination of trace rhodium in water samples with satisfactory results.
[Mh] Termos MeSH primário: Compostos de Anilina/química
Quelantes/química
Grafite/química
Ródio/análise
Espectrofotometria Atômica/métodos
Poluentes Químicos da Água/análise
[Mh] Termos MeSH secundário: Calibragem
Concentração de Íons de Hidrogênio
Limite de Detecção
Polietilenoglicóis
Temperatura Ambiente
Fatores de Tempo
[Pt] Tipo de publicação:JOURNAL ARTICLE
[Nm] Nome de substância:
0 (2-(5-iodo-2-pyridylazo)-5-dimethylaminoaniline); 0 (Aniline Compounds); 0 (Chelating Agents); 0 (Water Pollutants, Chemical); 30IQX730WE (Polyethylene Glycols); 7782-42-5 (Graphite); 9036-19-5 (Nonidet P-40); DMK383DSAC (Rhodium)
[Em] Mês de entrada:1705
[Cu] Atualização por classe:170523
[Lr] Data última revisão:
170523
[Sb] Subgrupo de revista:IM
[Da] Data de entrada para processamento:170325
[St] Status:MEDLINE


  5 / 2705 MEDLINE  
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[PMID]:28315002
[Au] Autor:Rinkovec J; Pehnec G; Zuzul S; Roncevic S
[Ad] Endereço:Institute for Medical Research and Occupational Health, Ksaverska cesta 2, 10001, Zagreb, Croatia. jrinkovec@imi.hr.
[Ti] Título:Determination of Platinum Group Elements in Particulate Matter by Inductively Coupled Plasma Mass Spectrometry.
[So] Source:Bull Environ Contam Toxicol;98(5):672-676, 2017 May.
[Is] ISSN:1432-0800
[Cp] País de publicação:United States
[La] Idioma:eng
[Ab] Resumo:This study examined a method for determination of rhodium (Rh), palladium (Pd) and platinum (Pt) in particulate matter using standard solutions, model samples and certified reference materials (NIST 1648a and ERM CZ120). The method was based on microwave digestion followed by inductively coupled plasma mass spectrometry (ICP-MS). The results showed that the stability of the standard solution mixture of Rh, Pd and Pt was better when chlorides were present in the solution. A membrane filter and one type of quartz filter were the most adequate for analyzing platinum group elements (PGE). Respective limits of detection for Rh, Pd and Pt were 0.028, 0.503 and 0.0265 pg/m with a membrane filter and 0.478, 4.530 and 0.070 pg/m for one type of quartz filters. The sample matrix had no significant effects on the determination of three PGEs.
[Mh] Termos MeSH primário: Espectrometria de Massas
Material Particulado/química
Platina/análise
[Mh] Termos MeSH secundário: Limite de Detecção
Paládio/análise
Ródio/análise
[Pt] Tipo de publicação:JOURNAL ARTICLE
[Nm] Nome de substância:
0 (Particulate Matter); 49DFR088MY (Platinum); 5TWQ1V240M (Palladium); DMK383DSAC (Rhodium)
[Em] Mês de entrada:1706
[Cu] Atualização por classe:170609
[Lr] Data última revisão:
170609
[Sb] Subgrupo de revista:IM
[Da] Data de entrada para processamento:170319
[St] Status:MEDLINE
[do] DOI:10.1007/s00128-017-2061-2


  6 / 2705 MEDLINE  
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[PMID]:28254039
[Au] Autor:Cao Y; Ran R; Wu X; Zhao B; Weng D
[Ad] Endereço:Key Laboratory of Advanced Materials, Ministry of Education, School of Materials Science and Engineering, Tsinghua University, Beijing 100084, China. Electronic address: yidanlily@gmail.com.
[Ti] Título:Improved activity and durability of Rh-based three-way catalyst under diverse aging atmospheres by ZrO support.
[So] Source:J Environ Sci (China);52:197-203, 2017 Feb.
[Is] ISSN:1001-0742
[Cp] País de publicação:Netherlands
[La] Idioma:eng
[Ab] Resumo:The catalytic activity and durability of Rh/ZrO catalyst were investigated compared with Rh/Al O catalyst under diverse aging atmospheres, including lean, rich and lean-rich cyclic aging atmospheres, to simulate the real working conditions of three-way catalyst. Oxidation states and microstructures of rhodium species were investigated to correlate with the catalytic performance of the catalysts. The catalytic performance and durability of the Rh catalyst under diverse aging atmospheres were drastically enhanced by ZrO support. ZrO support was confirmed to be able to effectively inhibit rhodium sintering even under diverse aging conditions. It can also successfully keep Rh species in an active low-valence state on the surface of the catalyst. The superiority of ZrO support compared to Al O was verified by the Rh-based monolith catalyst.
[Mh] Termos MeSH primário: Modelos Químicos
Ródio/química
Óxido de Zinco/química
[Mh] Termos MeSH secundário: Atmosfera
Catálise
Oxirredução
[Pt] Tipo de publicação:JOURNAL ARTICLE
[Nm] Nome de substância:
DMK383DSAC (Rhodium); SOI2LOH54Z (Zinc Oxide)
[Em] Mês de entrada:1703
[Cu] Atualização por classe:170324
[Lr] Data última revisão:
170324
[Sb] Subgrupo de revista:IM
[Da] Data de entrada para processamento:170304
[St] Status:MEDLINE


  7 / 2705 MEDLINE  
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[PMID]:28222978
[Au] Autor:Zimmermann S; Wolff C; Sures B
[Ad] Endereço:Aquatic Ecology, and Centre for Water and Environmental Research (CWE), University of Duisburg-Essen, Universitaetsstrasse 2, 45141 Essen, Germany. Electronic address: sonja.zimmermann@uni-due.de.
[Ti] Título:Toxicity of platinum, palladium and rhodium to Daphnia magna in single and binary metal exposure experiments.
[So] Source:Environ Pollut;224:368-376, 2017 May.
[Is] ISSN:1873-6424
[Cp] País de publicação:England
[La] Idioma:eng
[Ab] Resumo:Mainly due to automobile traffic, but also due to other sources, the platinum group elements (PGE) platinum (Pt), palladium (Pd) and rhodium (Rh) are introduced into aquatic biotopes where they accumulate in sediments of lakes and rivers. However, the toxicity of these noble metals to aquatic organisms is not well understood and especially toxicity studies under standardized condition are lacking. Thus, the toxicity of Pt, Pd and Rh to Daphnia magna was tested in single metal exposure experiments according to OECD guideline 202. Immobility and lethality was recorded after 24 h and 48 h of exposure and EC and LC , respectively, were determined. As the nominal exposure concentration of Pd differed significantly from the quantified concentration, the control of the real exposure concentration by chemical analysis is mandatory, especially for Pd. The toxicity decreased in the order Pd > Pt â‰« Rh with e.g. LC (48 h) values of 14 µg/L for Pd, 157 µg/L for Pt and 56,800 µg/L for Rh. The exposure period had a clear effect on the toxicity of Pt, Pd and Rh. For Pt and Rh the endpoint immobility was more sensitive than the endpoint lethality whereas Pd toxicity was similar for both endpoints. The Hill slopes, which are a measure for the steepness of the concentration-response curves, showed no significant discrepancies between the different metals. The binary metal exposure to Pt and Pd revealed a more-than-additive, i.e. a synergistic toxicity using the toxic unit approach. The present study is a start to understand the toxicity of interacting PGE. The modes of action behind the synergistic effect are unclear.
[Mh] Termos MeSH primário: Daphnia/efeitos dos fármacos
Platina/toxicidade
Ródio/toxicidade
Rios/química
Emissões de Veículos/análise
Poluentes Químicos da Água/análise
[Mh] Termos MeSH secundário: Animais
Monitoramento Ambiental
Paládio
[Pt] Tipo de publicação:JOURNAL ARTICLE
[Nm] Nome de substância:
0 (Vehicle Emissions); 0 (Water Pollutants, Chemical); 49DFR088MY (Platinum); 5TWQ1V240M (Palladium); DMK383DSAC (Rhodium)
[Em] Mês de entrada:1705
[Cu] Atualização por classe:170522
[Lr] Data última revisão:
170522
[Sb] Subgrupo de revista:IM
[Da] Data de entrada para processamento:170223
[St] Status:MEDLINE


  8 / 2705 MEDLINE  
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[PMID]:28219005
[Au] Autor:Yang C; Wang W; Liang JX; Li G; Vellaisamy K; Wong CY; Ma DL; Leung CH
[Ad] Endereço:State Key Laboratory of Quality Research in Chinese Medicine, Institute of Chinese Medical Sciences, University of Macau , Macau, China.
[Ti] Título:A Rhodium(III)-Based Inhibitor of Lysine-Specific Histone Demethylase 1 as an Epigenetic Modulator in Prostate Cancer Cells.
[So] Source:J Med Chem;60(6):2597-2603, 2017 Mar 23.
[Is] ISSN:1520-4804
[Cp] País de publicação:United States
[La] Idioma:eng
[Ab] Resumo:We report herein a novel rhodium(III) complex 1 as a new LSD1 targeting agent and epigenetic modulator. Complex 1 disrupted the interaction of LSD1-H3K4me2 in human prostate carcinoma cells and enhanced the amplification of p21, FOXA2, and BMP2 gene promoters. Complex 1 was selective for LSD1 over other histone demethylases, such as KDM2b, KDM7, and MAO activities, and also showed antiproliferative activity toward human cancer cells. To date, complex 1 is the first metal-based inhibitor of LSD1 activity.
[Mh] Termos MeSH primário: Antineoplásicos/farmacologia
Complexos de Coordenação/farmacologia
Histona Desmetilases/antagonistas & inibidores
Próstata/efeitos dos fármacos
Neoplasias da Próstata/tratamento farmacológico
Ródio/farmacologia
[Mh] Termos MeSH secundário: Antineoplásicos/química
Linhagem Celular Tumoral
Proliferação Celular/efeitos dos fármacos
Complexos de Coordenação/química
Epigênese Genética/efeitos dos fármacos
Regulação Neoplásica da Expressão Gênica/efeitos dos fármacos
Histona Desmetilases/metabolismo
Seres Humanos
Masculino
Simulação de Acoplamento Molecular
Próstata/metabolismo
Próstata/patologia
Neoplasias da Próstata/genética
Neoplasias da Próstata/metabolismo
Neoplasias da Próstata/patologia
Ródio/química
[Pt] Tipo de publicação:JOURNAL ARTICLE
[Nm] Nome de substância:
0 (Antineoplastic Agents); 0 (Coordination Complexes); DMK383DSAC (Rhodium); EC 1.14.11.- (Histone Demethylases); EC 1.5.- (KDM1A protein, human)
[Em] Mês de entrada:1706
[Cu] Atualização por classe:170619
[Lr] Data última revisão:
170619
[Sb] Subgrupo de revista:IM
[Da] Data de entrada para processamento:170221
[St] Status:MEDLINE
[do] DOI:10.1021/acs.jmedchem.7b00133


  9 / 2705 MEDLINE  
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[PMID]:28035818
[Au] Autor:Martin SC; Vohidov F; Wang H; Knudsen SE; Marzec AA; Ball ZT
[Ad] Endereço:Department of Chemistry, Rice University , Houston, Texas 77005, United States.
[Ti] Título:Designing Selectivity in Dirhodium Metallopeptide Catalysts for Protein Modification.
[So] Source:Bioconjug Chem;28(2):659-665, 2017 Feb 15.
[Is] ISSN:1520-4812
[Cp] País de publicação:United States
[La] Idioma:eng
[Ab] Resumo:The ability to chemically alter proteins is important for broad areas of chemical biology, biophysics, and medicine. Chemical catalysts for protein modification, and particularly rhodium(II) conjugates, represent an important new approach to protein modification that develops novel functionalization approaches while shedding light on the development of selective chemistries in complex environments. Here, we elucidate the reaction parameters that allow selective catalysis and even discrimination among highly similar proteins. Furthermore, we show that quantifying modification allows the measurement of competitive ligand affinity, permitting straightforward measurement of protein-peptide interactions and inhibitors thereof. Taken as a whole, rhodium(II) conjugates replicate many features of enzymes in an entirely chemical construct.
[Mh] Termos MeSH primário: Peptídeos/química
Proteínas/química
Ródio/química
[Mh] Termos MeSH secundário: Alquinos/química
Sequência de Aminoácidos
Compostos Azo/química
Biotina/química
Catálise
Seres Humanos
Proteína Tirosina Quinase p56(lck) Linfócito-Específica/química
Modelos Moleculares
Espectrometria de Massas por Ionização e Dessorção a Laser Assistida por Matriz
Domínios de Homologia de src
[Pt] Tipo de publicação:JOURNAL ARTICLE
[Nm] Nome de substância:
0 (Alkynes); 0 (Azo Compounds); 0 (Peptides); 0 (Proteins); 6SO6U10H04 (Biotin); DMK383DSAC (Rhodium); EC 2.7.10.2 (Lymphocyte Specific Protein Tyrosine Kinase p56(lck))
[Em] Mês de entrada:1706
[Cu] Atualização por classe:170607
[Lr] Data última revisão:
170607
[Sb] Subgrupo de revista:IM
[Da] Data de entrada para processamento:161231
[St] Status:MEDLINE
[do] DOI:10.1021/acs.bioconjchem.6b00716


  10 / 2705 MEDLINE  
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[PMID]:27997743
[Au] Autor:Streciwilk W; Terenzi A; Misgeld R; Frias C; Jones PG; Prokop A; Keppler BK; Ott I
[Ad] Endereço:Institute of Medicinal and Pharmaceutical Chemistry, Technische Universität Braunschweig, Beethovenstr. 55, 38106, Braunschweig, Germany.
[Ti] Título:Metal NHC Complexes with Naphthalimide Ligands as DNA-Interacting Antiproliferative Agents.
[So] Source:ChemMedChem;12(3):214-225, 2017 Feb 03.
[Is] ISSN:1860-7187
[Cp] País de publicação:Germany
[La] Idioma:eng
[Ab] Resumo:Naphthalimide-based N-heterocyclic carbene (NHC) complexes of the type [(1,5-cyclooctadiene)(NHC)RhCl)] (4 a-c), [(p-cymene)(NHC)RuCl )] (5 a-c), and [(NHC)CuBr] (6 a-c) were synthesized and investigated as antiproliferative agents that target DNA. The cytotoxic effects were largely driven by the naphthalimide structure, which is a DNA-intercalating moiety. Regarding the metal center, the highest activities were observed with the rhodium complexes, and cytotoxic activity was significantly lower for the ruthenium derivatives. The stable coordination of the NHC ligands of selected complexes 4 b and 5 b in solution was confirmed, and their DNA binding properties were studied by UV/Vis spectroscopy, mass spectrometry, and circular dichroism. Stable intercalative binding into the DNA for all selected naphthalimide-based complexes is indicated by high DNA binding constants. Particularly efficient binding was observed in the case of the rhodium complex 4 b. More detailed biological studies on 4 b showed promising activities against multidrug-resistant Nalm-6 cells and confirmed an important role for mitochondrial pathways in 4 b-induced apoptosis.
[Mh] Termos MeSH primário: Complexos de Coordenação/química
DNA/química
Substâncias Intercalantes/química
Metano/análogos & derivados
Naftalimidas/química
[Mh] Termos MeSH secundário: Apoptose/efeitos dos fármacos
Proliferação Celular/efeitos dos fármacos
Dicroísmo Circular
Complexos de Coordenação/síntese química
Complexos de Coordenação/toxicidade
Cristalografia por Raios X
DNA/metabolismo
Estabilidade de Medicamentos
Células HT29
Seres Humanos
Substâncias Intercalantes/síntese química
Substâncias Intercalantes/toxicidade
Ligantes
Células MCF-7
Metano/química
Conformação Molecular
Monoterpenos/química
Ródio/química
Rutênio/química
Espectrofotometria Ultravioleta
[Pt] Tipo de publicação:JOURNAL ARTICLE
[Nm] Nome de substância:
0 (Coordination Complexes); 0 (Intercalating Agents); 0 (Ligands); 0 (Monoterpenes); 0 (Naphthalimides); 1G1C8T1N7Q (4-cymene); 2465-56-7 (carbene); 7UI0TKC3U5 (Ruthenium); 9007-49-2 (DNA); DMK383DSAC (Rhodium); OP0UW79H66 (Methane)
[Em] Mês de entrada:1706
[Cu] Atualização por classe:170630
[Lr] Data última revisão:
170630
[Sb] Subgrupo de revista:IM
[Da] Data de entrada para processamento:161221
[St] Status:MEDLINE
[do] DOI:10.1002/cmdc.201600557



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